Prep HPLC Column, Diol, 4um, 100A. 30mm ID x 250mm Length. Cogent TYPE-C Brand. 1 EA.

Additional Info:

The 40060‑P30‑250 Diol Preparative HPLC Column is engineered for high‑capacity, high‑resolution preparative purification workflows where shorter or smaller‑diameter columns no longer provide sufficient separation, peak capacity, or loading tolerance. Manufactured with 4 µm, 100 Å Cogent TYPE‑C™ silica hydride, this column enables efficient isolation and collection of large milligram‑to‑gram‑level quantities of polar and amine‑containing compounds while maintaining the selectivity and retention behavior fundamental to Diol chromatography.

The extended column length provides maximum resolving power, making this column ideal for demanding, late‑stage purification of complex polar mixtures.

Preparative Use Case: Why 30 mm ID × 250 mm

The 30 mm internal diameter classifies this column as large‑scale preparative, enabling very high sample loading and large‑volume fraction collection. Compared with 21.2 mm and shorter 30 mm formats, this configuration:

  • Supports very high sample loads

  • Enables collection of large, clean fractions

  • Preserves chromatographic selectivity during scale‑up

  • Supports production‑scale and late‑stage purification workflows

The 250 mm column length delivers the highest resolution and peak capacity in the Diol preparative series, making it the preferred choice for separating closely eluting or structurally similar polar compounds where maximum separation confidence is required.

Diol TYPE‑C™ Stationary Phase Advantages

Manufactured using Cogent TYPE‑C™ silica hydride technology, the Diol stationary phase provides distinct advantages for large‑scale HILIC and normal‑phase purification:

  • Excellent selectivity for polar and amine‑containing compounds

  • Faster equilibration than conventional bonded‑silica Diol phases

  • Robust column lifetime, even under extended high‑organic mobile‑phase conditions

This chemistry is particularly well suited for purification of:

  • Metabolites

  • Polar small molecules

  • Analytes containing amine or basic functional groups

  • Compounds with poor retention using reversed‑phase chromatography

Made‑to‑Order Columns & Pricing Information

Large‑diameter preparative columns are application‑specific tools and represent a significant investment. To ensure correct configuration and compatibility:

  • Columns are manufactured to order

  • Orders cannot be returned or canceled once placed

  • Pricing and technical guidance are provided by Customer Service via formal quotation

System Requirements

  • Typical operating flow rates: ~20–50 mL/min

  • Requires a large‑scale preparative HPLC system capable of:

    • High‑flow solvent delivery

    • Very large injection volumes

    • Industrial‑grade detectors and fraction‑collection systems

Analytical and semi‑preparative HPLC systems are not suitable for 30 mm ID preparative columns.

Flow rates should be optimized based on mobile‑phase viscosity, system pressure limits, and purification objectives.

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